Lucky7's,
Don't waste time boiling the oil with water. The temperature will only rise to 212F until the water is mostly gone, and boiling large amounts of water under oil can cause steam explosions that are messy and dangerous. Boiling oil with water also causes hydrolysis that will likely result in the loss of some glycerol.
You can:
1. Centrifuge, or fine filter the oil to remove sediments.
2. Gently water wash the oil to remove any remaining water soluble contaminants (avoid creating an emulsion).
3. Heat the wet oil to 350F to ensure all is dead that remains.
4. Conduct a Sap test to determine the amount of caustic necessary.
5. Make your soap using your determined Sap value.
Edit:
Forgot to add,
Refining glycerol/glycerin, is done using vacuum distillation due to it's boiling point being it's decomposition temperature.
My appologies for jumping in with advice after just joining, I hope no one takes offense.
Don't waste time boiling the oil with water. The temperature will only rise to 212F until the water is mostly gone, and boiling large amounts of water under oil can cause steam explosions that are messy and dangerous. Boiling oil with water also causes hydrolysis that will likely result in the loss of some glycerol.
You can:
1. Centrifuge, or fine filter the oil to remove sediments.
2. Gently water wash the oil to remove any remaining water soluble contaminants (avoid creating an emulsion).
3. Heat the wet oil to 350F to ensure all is dead that remains.
4. Conduct a Sap test to determine the amount of caustic necessary.
5. Make your soap using your determined Sap value.
Edit:
Forgot to add,
Refining glycerol/glycerin, is done using vacuum distillation due to it's boiling point being it's decomposition temperature.
My appologies for jumping in with advice after just joining, I hope no one takes offense.