RacerSpuffy
Active Member
- Joined
- Dec 28, 2017
- Messages
- 26
- Reaction score
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I decided to get into soap making for a few reasons, the biggest reason is that I hoped to make some soap that would help with seasonal dry skin. For much less important reasons I thought it might be cool to give some away to my family and friends. I'm not looking to do this on any large scale or go into selling. Hobby/curiosity and not a job
I have a fair bit of experience both in graduate school and in professional life working with very concentrated acids and bases so I was comfortable with CP soap making. In fact, I thought I was comfortable with HP too but after watching some videos on that I've decided I won't attempt that until summer time and I can do it outside.
Everything I have made so far has gone into a 6 bar 4oz/bar silicon mold.
On to what I have done and my questions:
Batch 1:This was a very 'fly by the seat of my pants' type make. I use SoapCalc and didn't pay any attention to the ranges suggested to stay within, I also didn't really think things through on the volume I was making and came up a bit short at only 3.75 bars.
Ingredients:
Coconut Oil (76) - 227g (80%)
Olive Oil - 57g (20%)
Lye - 47g
Distilled Water - 108g
I did this with a cheap scale, so while SoapCalc gave me to decimal places I just rounded to nearest gram. I also don't have a stick blender/immersion blender so I just hand whisked it.
I mixed the oils into the lye water when both were at about 115F. I whisked by hand while keeping the temp between 115 and 130F as read by an IR temp gun. After about 45 minutes I was getting a pretty decent trace and I dumped in a bit of wet coffee grounds (for 2 reasons, one was I wanted a bit of 'pumice' to it and also thought it might kill the garlic scent that turns out my olive oil had in it). I poured into the mold and the last 0.75 bars had to be removed with a spatula since it was about the consistency of pudding at this point. I then covered with plastic wrap and a light towel. 16 hours later I removed the bars and was pretty happy with them.
Batch 2: Was so pleased at how simple things worked on Batch 1 I went out and got some more ingredients and scaled things up enough to fill all 6 slots in my mold.
Ingredients:
Morrell Snow Cap Manteca (Lard) - 200g (50%)
Kroger Pure Canola Oil - 100g (25%)
Coconut Oil - 100g (25%)
Sodium Hydroxide - 57g
Distilled Water - 152g
Mixed at same temperatures as batch 1, hand whisked. Took forever to get to trace, in fact I'm not sure it really ever did what I'd consider a trace. However I'm certain there wasn't any separation of oil and lye-water after 30 min (probably sooner). It got to perhaps a weak trace at 110 minutes of whisking and frankly I was tired of dealing with it at this point. I added a small amount of essential oils (guessing about 0.05g) so I poured it and covered like Batch 1.
On removing from the mold ~20 hours later, a bit stuck in the corners but whatever it came out mostly good. Much whiter than Batch 1, but I used different oils and didn't add any coffee so figured thats how it should be.
Batch 3: Ok, at this point I realized my numbers are way out of suggested range for Batch 1, and Batch 2 just by luck seemed to fit in the number ranges on SoapCalc just fine. I also have read a bit more at this point and attribute the slow trace time to the low lye concentration in Batch 2. So I decide I'm going to bump my lye concentration up to 35% for this one. I play around with SoapCalc and different fat sources again and decide on 4 sources.
Ingredients:
Morrell Snow Cap Manteca (Lard) - 120g (30%)
Kroger All Vegetable Shortening - 120g (30%)
Coconut Oil - 120g (30%)
Filippo Berio Olive Oil - 40g (10%)
Sodium Hydroxide - 56g
Distilled Water - 104g
Mix at same temps as Batch 1 and 2, but this time I have decided I don't want to hand whisk for 2 hours anymore. I also didn't want to spend $30 for an immersion blender, so I bought an 88 cent whisk and cut the hanging loop off the end and mounted it in my drill. Expecting a fast trace because I used higher lye concentration and am now mechanically stirring rather than by hand. After an hour and a half of no trace or extremely minimal I give up because I have somewhere to be, so I add a tiny bit of food coloring (that was gel type and didn't mix well, but actually the result was kinda cool) and the same amount and same type of essential oil as before. Pour in mold, cover as before. 20h later I remove from mold and it breaks up a bit more on the edges than batch 2 which is somewhat concerning but I'm not terribly upset.
Batch 4: I'm not happy with the long time to trace and I'm not crazy about how much bar is sticking in the corners/edges of the mold - its not terrible, but after how well the first ones came out I'm disappointed. So, with that in mind and knowing now about wanting to keep the soap qualities in the suggested ranges I find that if I essentially flip the oil amounts around from Batch 1 I can get a more rounded bar. Also based on my experience thus far I figure it I can probably take it to family over Christmas and even though I know it isn't ready to be used, I could probably give a few bars out and tell them it still needs to dry/cure. So I set forth with this:
Ingredients:
Filippo Berio Olive Oil - 338g (75%)
Coconut Oil - 113g (25%)
Sodium Hydroxide - 63g
Distilled Water - 117g
Mix just like what I did with previous batches. This time I mix by hand again based on time to trace not being improved with drill whisking, I figure I'll try and speed this up by mixing at 120-130F. After an hour and a half of whisking I get discouraged, and pour it into the mold. I figure its fine, the earlier ones didn't trace well either and I had no separation issues. I had this in a box that nearly perfectly fit my mold so I cover with aluminum foil, and then wrap the box in a couple towels and let sit for ~4 hours. Then its time to travel, I didn't peek at the soap because it didn't matter, I wanted to bring this to family so it was going to work or not, peeking wasn't going to change anything. I transport it, bring it inside when I get where I'm going and it sits 24 hours before I look at it. When I look at it, some of it slopped around during transport but its mostly ok, however it is way too soft to remove from the mold. I attribute this to the room temperature being about 57F rather than ~68 that my other soaps were at. 48 hours later I am able to remove it, and there is a more white base and the top half is more 'wet' looking. I still don't see any oil/water separation so I figure it is probably ok.
My concerns/questions:
Is what I've described typical for the blends I made?
Why does Batch 1 look different (aside from the coffee)? - batch 1 looks like maybe it partially gelled, but not actually sure that happened.
Batches 2-4 are all a bit crumbly on removal from the mold, batch 1 was not.
Why did Batch 1 thicken up like I expected based on what I'd seen in youtube videos from various people but Batches 2-4 not?
Is the stick blender the key here on getting to trace faster? Is 90+ minutes typical?
I know this is a huge first post for a newbie. If there is anything more you want to know just ask. I did create a spreadsheet for each of these, including bar weights so I could monitor drying over time.
I have a fair bit of experience both in graduate school and in professional life working with very concentrated acids and bases so I was comfortable with CP soap making. In fact, I thought I was comfortable with HP too but after watching some videos on that I've decided I won't attempt that until summer time and I can do it outside.
Everything I have made so far has gone into a 6 bar 4oz/bar silicon mold.
On to what I have done and my questions:
Batch 1:This was a very 'fly by the seat of my pants' type make. I use SoapCalc and didn't pay any attention to the ranges suggested to stay within, I also didn't really think things through on the volume I was making and came up a bit short at only 3.75 bars.
Ingredients:
Coconut Oil (76) - 227g (80%)
Olive Oil - 57g (20%)
Lye - 47g
Distilled Water - 108g
I did this with a cheap scale, so while SoapCalc gave me to decimal places I just rounded to nearest gram. I also don't have a stick blender/immersion blender so I just hand whisked it.
I mixed the oils into the lye water when both were at about 115F. I whisked by hand while keeping the temp between 115 and 130F as read by an IR temp gun. After about 45 minutes I was getting a pretty decent trace and I dumped in a bit of wet coffee grounds (for 2 reasons, one was I wanted a bit of 'pumice' to it and also thought it might kill the garlic scent that turns out my olive oil had in it). I poured into the mold and the last 0.75 bars had to be removed with a spatula since it was about the consistency of pudding at this point. I then covered with plastic wrap and a light towel. 16 hours later I removed the bars and was pretty happy with them.
Batch 2: Was so pleased at how simple things worked on Batch 1 I went out and got some more ingredients and scaled things up enough to fill all 6 slots in my mold.
Ingredients:
Morrell Snow Cap Manteca (Lard) - 200g (50%)
Kroger Pure Canola Oil - 100g (25%)
Coconut Oil - 100g (25%)
Sodium Hydroxide - 57g
Distilled Water - 152g
Mixed at same temperatures as batch 1, hand whisked. Took forever to get to trace, in fact I'm not sure it really ever did what I'd consider a trace. However I'm certain there wasn't any separation of oil and lye-water after 30 min (probably sooner). It got to perhaps a weak trace at 110 minutes of whisking and frankly I was tired of dealing with it at this point. I added a small amount of essential oils (guessing about 0.05g) so I poured it and covered like Batch 1.
On removing from the mold ~20 hours later, a bit stuck in the corners but whatever it came out mostly good. Much whiter than Batch 1, but I used different oils and didn't add any coffee so figured thats how it should be.
Batch 3: Ok, at this point I realized my numbers are way out of suggested range for Batch 1, and Batch 2 just by luck seemed to fit in the number ranges on SoapCalc just fine. I also have read a bit more at this point and attribute the slow trace time to the low lye concentration in Batch 2. So I decide I'm going to bump my lye concentration up to 35% for this one. I play around with SoapCalc and different fat sources again and decide on 4 sources.
Ingredients:
Morrell Snow Cap Manteca (Lard) - 120g (30%)
Kroger All Vegetable Shortening - 120g (30%)
Coconut Oil - 120g (30%)
Filippo Berio Olive Oil - 40g (10%)
Sodium Hydroxide - 56g
Distilled Water - 104g
Mix at same temps as Batch 1 and 2, but this time I have decided I don't want to hand whisk for 2 hours anymore. I also didn't want to spend $30 for an immersion blender, so I bought an 88 cent whisk and cut the hanging loop off the end and mounted it in my drill. Expecting a fast trace because I used higher lye concentration and am now mechanically stirring rather than by hand. After an hour and a half of no trace or extremely minimal I give up because I have somewhere to be, so I add a tiny bit of food coloring (that was gel type and didn't mix well, but actually the result was kinda cool) and the same amount and same type of essential oil as before. Pour in mold, cover as before. 20h later I remove from mold and it breaks up a bit more on the edges than batch 2 which is somewhat concerning but I'm not terribly upset.
Batch 4: I'm not happy with the long time to trace and I'm not crazy about how much bar is sticking in the corners/edges of the mold - its not terrible, but after how well the first ones came out I'm disappointed. So, with that in mind and knowing now about wanting to keep the soap qualities in the suggested ranges I find that if I essentially flip the oil amounts around from Batch 1 I can get a more rounded bar. Also based on my experience thus far I figure it I can probably take it to family over Christmas and even though I know it isn't ready to be used, I could probably give a few bars out and tell them it still needs to dry/cure. So I set forth with this:
Ingredients:
Filippo Berio Olive Oil - 338g (75%)
Coconut Oil - 113g (25%)
Sodium Hydroxide - 63g
Distilled Water - 117g
Mix just like what I did with previous batches. This time I mix by hand again based on time to trace not being improved with drill whisking, I figure I'll try and speed this up by mixing at 120-130F. After an hour and a half of whisking I get discouraged, and pour it into the mold. I figure its fine, the earlier ones didn't trace well either and I had no separation issues. I had this in a box that nearly perfectly fit my mold so I cover with aluminum foil, and then wrap the box in a couple towels and let sit for ~4 hours. Then its time to travel, I didn't peek at the soap because it didn't matter, I wanted to bring this to family so it was going to work or not, peeking wasn't going to change anything. I transport it, bring it inside when I get where I'm going and it sits 24 hours before I look at it. When I look at it, some of it slopped around during transport but its mostly ok, however it is way too soft to remove from the mold. I attribute this to the room temperature being about 57F rather than ~68 that my other soaps were at. 48 hours later I am able to remove it, and there is a more white base and the top half is more 'wet' looking. I still don't see any oil/water separation so I figure it is probably ok.
My concerns/questions:
Is what I've described typical for the blends I made?
Why does Batch 1 look different (aside from the coffee)? - batch 1 looks like maybe it partially gelled, but not actually sure that happened.
Batches 2-4 are all a bit crumbly on removal from the mold, batch 1 was not.
Why did Batch 1 thicken up like I expected based on what I'd seen in youtube videos from various people but Batches 2-4 not?
Is the stick blender the key here on getting to trace faster? Is 90+ minutes typical?
I know this is a huge first post for a newbie. If there is anything more you want to know just ask. I did create a spreadsheet for each of these, including bar weights so I could monitor drying over time.