Getting ready to make my first liquid soap

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DawninWA

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I've been making soap for 4 years, and I want to venture into liquid soap. I have 2 lbs of KOH coming on Friday.

I want to use Palm Kernel Oil flakes, HO Safflower oil, and shea butter. I also have olive oil, coconut oil, Great Value shortening, cocoa butter, palm oil and lard, I'd rather not use lard.

Should I add other oils besides the first 3? And I don't know what percentages of the three I should do. I like high coconut in bars, we have hard water here. Should the PKO be pretty high? Can I go up to 40 or 50%?

Something like:
40% PKO
50% Safflower
10% Shea
3% superfat (2%? I don't know)
?

Any red flags with this recipe? Anything else I should be considering? I'm using PKO instead of Coconut because my skin can be sensitive to coconut, and I have a bunch (of PKO) I'd like to use up. I also don't care if it's cloudy or whatnot.

I'm planning to do cold process with water, it looks the easiest.

Thank you!
Dawn
 
I've only made a couple of batches of LS, but as I understand it you cannot superfat unless it is a water soluble oil such as red turkey. If you do superfat then once the LS sits for a bit the excess oil floats to the top. I guess that is OK as long as you or the final consumer remembers to shake the bottle each time you use it. As to the recipe itself I don't know enough to comment. Good luck.
 
That's my experience too -- superfatting at 3% or under is generally okay. If you superfat higher than that, it is likely to not work. If the superfat separates out, you may have to use polysorbate to emulsify/solubilize the fat or switch to a water-soluble fat (turkey red oil being an example.)
 
Are you using regular safflower or high oleic safflower?

If HO saff, it's not too bad of a recipe. There's going to be enough oleic acid so you can dilute it to a honey-thick soap. It's probably going to be more cleansing/stripping than I'd prefer, but that's a personal preference.

If regular (high linoleic) safflower, the soap is going to be more prone to rancidity. You may not be able to dilute it to a honey-thick consistency due to less oleic acid -- it may be thinner than you might want.

Refined shea may add cloudiness. Unrefined may add sediments that will settle out over time. You said cloudiness wasn't a deal killer for you, so this is a moot point.
 
I wrote in the first paragraph (edit to add: sorry, second paragraph) that it was HO, but I didn't when I wrote out the recipe, I'll remember to do that in the future.

I use it in place of olive oil in my bar soap, and I like it a little better.

Thank you, DeeAnna. That was very helpful!
 
Well, darn, my lye order got delayed. Amazon says it could still be here today, but UPS tracking says it was in Portland this morning, and it's unlikely.

I'm going to do less PKO, since I won't have that superfat to lean on. Maybe just 20% PKO, 80% HO Safflower.

How well do animal fats work in liquid soap? I love using the walmart shortening in soap, but I don't often use it in soaps I sell, because there are a lot of ingredients that scare people. I also have a lot of it. Can I use mostly this? Like 20% PKO, 80% shortening? It's mostly tallow, a little palm, and some BHA, BHT, and some other stabilizers. I assume this would be cloudy.

I'm also going to make a batch of 100% coconut for cleaning. This would use less water to dilute, right, more of a 1:1?

Then I can experiment with butters later.
 
I've made liquid soap with 70% lard. Even when I added enough KOH to make the soap stay slightly lye heavy (slight zap), it wanted to separate into a white floating layer and a clear bottom layer. I'm not sure why, but my guess is the high % of stearic and palmitic acids. These fatty acids make soap that's not very soluble in water. Not sure if I'm right about that, but that's the best explanation I can think of at this point. The soap was nearly colorless like water -- not amber like typical liquid soap -- after I skimmed off the floating layer. It was nice enough soap to use for handwashing (after I got rid of the excess KOH).
 
That must be why most liquid soap is vegetable based.

I took this extra few days (I'm assuming the lye will be here Monday), to infuse some herbs into the safflower oil. I don't know if any of the properties will survive the lye, but it's fun.
 
That must be why most liquid soap is vegetable based....

I would state this conclusion a little differently. Many liquid soap recipes for body use are some variation of coconut oil, olive, and castor. These recipes typically minimize or eliminate the palmitic and stearic fats such as palm, tallow, lard, and the butters (cocoa, shea, etc.) One reason for this is the desire for a clear soap, but a related reason is a greater chance for separation, if my guess is right.
 
20180910_194918.jpg


Here goes nothing. Decided on 30% pko, 65% HO safflower, 5% shea butter. 1% superfat. Traced really fast, let it sit, turned into what's in the photo after 25 minutes. Not sure if it's done and cloudy because of the shea, or not done yet. I'll leave it alone for about an hour and then zap test. If it passes, I'll add 1:1 water and leave it until tomorrow.

Well, I was impatient, I decided to zap test. It passed. That was all very fast, and about the easiest soap I've ever made.
 
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It's almost done diluting. I started with 25 oz of paste, first I added 25 oz of distilled water, then 10, then in 5 oz increments and now it's at 2:1. It's almost there, I'll add in tiny increments from here on out. I like the recipe, it's not drying but is cleansing.

I'm in the process of making another batch, it stopped separating and I'm just waiting for it to gel. It is 100% coconut oil 0% superfat, for dishes.

20180911_171742.jpg

We have soap!
 
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The coconut oil soap finished pretty fast, with no complications. I diluted some of it in a jar at 1:1 ratio. It worked fine.

I decided to do a batch of straight olive oil, and that was a little harder to do. It took forever to stay together. I started it at 4 pm last night, and at 8, I put it on the heat so it could cook and hopefully speed the process along. Eventually, it was staying together. At 5am, it had separated a little, but was mostly together. At noon, it was still together, but like a thick pudding. I left it alone until about 4 pm and it had gelled. It didn't zap, so I put some in a jar with water, also at a 1:1 ratio. I know it'll need more water, but I'll start with that.

Three batches of soap will keep me stocked for a long time, and having the different kinds will allow me to see how each one acts.
 

Hi I see you've scented the soap with several fragrances/EOs. did you add the Fragrance when diluting?. what about adding color.

Once I added water soluble color when making CPLS and let it sit for over month. I had some water separated from the soap paste together with the color. That's why I'm wondering which would be the best point to add color and fragrances. thank
 
I diluted the whole batch, put it in bottles, then added the essential oils to each bottle.

I have no idea about coloring the soap.
 
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